Experiments have been made in a laboratory heavy media separator at various specific gravities of separation using zinc chloride solution and magnetite suspension as media for different types of coals. The results indicate that the magnetite bath gives at better separation than zinc chloride solution. Even though the probable error remains the same for most conditions of operation, the error area is found to have a wide variation which emphasises the importance of the error area over probable error in evaluating the performance of a cleaning unit.