A synthetic gold-silver telluride material (mainly sylvanite) has been prepared and its physical and chemical properties checked. Flotation tests using a Hallimond tube were conducted using commercial xanthate collectors. At collector concentrations of 10-3M with the addition of 5 10-4 M CUS04, no obvious differences in the mineral recoveries were seen irrespective of whether amyl, secbutyl, isobutyl or isopropyl xanthates were used. However, when the concentration of xanthate was reduced to 10-4 M or in the absence of the copper sulphate activator, the effectiveness of the collectors was in the order: amyl > secbutyl > isobutyl > isopropyl > ethyl. Changes in the slurry pH appeared to have little effect on the recovery of the telluride mineral.Leaching tests of the precious metal telluride showed that both gold and silver dissolve in alkaline oxygenated cyanide solutions but at a much lower dissolution rate than metallic gold or silver. Both leaching tests and electrochemical measurements indicate that the dissolution rate of gold-silver telluride is controlled by the pH and cyanide concentration of the leachant.Roasting the gold-silver telluride materials in air at temperatures between 550 and 750C resulted in its decomposition into a metallic gold-silver alloy and tellurium dioxide.