This paper presents the results and findings of geochemical and mineralogical testwork conducted on samples collected from waste rock dumps at two mine sites, located in South Carolina, USA (Site 1) and Sudbury Ontario, Canada (Site 2). Important aspects of the relationship between the physical and geochemical aspects of the dumps are also presented. The overall aims of the project were to 1. determine if the physical and hydrological nature of the waste-rock dumps had any impact on the geochemical and mineralogical characteristics of the dump materials; and 2. to identify key implications for dump construction for ARD control. The results of geochemical and mineralogical tests indicate that the waste rock at Site 1 had undergone significant in-dump weathering and was relatively advanced with respect to ARD evolution. In contrast, the waste rock at Site 2 had undergone some weathering, however still contained a considerable amount of sulfide minerals. Testing also suggested that flushing of oxidation products at Site 2 had been limited, which therefore promoted the storage of oxidation products at the site. In addition, materials that had a D50 particle size in the range of 5 mm to 30 mm appeared to be more readily flushed than samples that had a D50 particle size of <5 mm or>30 mm. This suggested that preferential water pathways may have developed within the dumps at both sites.